Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7006278
Preview
Coordinates | 7006278.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C41 H52 P4 Pd |
---|---|
Calculated formula | C41 H52 P4 Pd |
SMILES | c1(c(cc(cc1C)C)C)P1P(c2c(cc(cc2C)C)C)[Pd]1([P](C)(C)c1ccccc1)[P](C)(C)c1ccccc1.c1(ccccc1)C |
Title of publication | Oxidative cleavage of tetraaryltetraphosphane-1,4-diides by nickel(II) and palladium(II): formation of unusual Ni(0) and Pd(0) diaryldiphosphene complexes. |
Authors of publication | Gómez-Ruiz, Santiago; Hey-Hawkins, Evamarie |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2007 |
Journal issue | 48 |
Pages of publication | 5678 - 5683 |
a | 11.3887 ± 0.0016 Å |
b | 12.423 ± 0.002 Å |
c | 15.829 ± 0.003 Å |
α | 84.327 ± 0.017° |
β | 72.773 ± 0.018° |
γ | 66.212 ± 0.016° |
Cell volume | 1956.8 ± 0.6 Å3 |
Cell temperature | 180 ± 2 K |
Ambient diffraction temperature | 180 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0469 |
Residual factor for significantly intense reflections | 0.0301 |
Weighted residual factors for significantly intense reflections | 0.0656 |
Weighted residual factors for all reflections included in the refinement | 0.0712 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.023 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7006278.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.