Information card for entry 7006666

Structure parameters

• Formula: C30 H46 N4 S Si4 Ta
• Calculated formula: C30 H37 N4 S Si4 Ta
• Title of publication: Olefination and group transfer reactions of an electron deficient tantalum methylidene complex.
• Authors of publication: Mullins, Sarah M.; Bergman, Robert G.; Arnold, John
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 1
• Pages of publication: 203 - 212
• a: 12.9195 ± 0.0003 Å
• b: 18.8911 ± 0.0004 Å
• c: 16.7243 ± 0.0002 Å
• α: 90°
• β: 103.423 ± 0.001°
• γ: 90°
• Cell volume: 3970.29 ± 0.13 ų
• Cell temperature: 168.2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0433
• Residual factor for significantly intense reflections: 0.0323
• Weighted residual factors for all reflections: 0.0438
• Weighted residual factors for all reflections included in the refinement: 0.0416
• Goodness-of-fit parameter for all reflections included in the refinement: 1.676
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No