Information card for entry 7006844

Structure parameters

• Formula: C224 H392 K6 N24 O8 Si12
• Calculated formula: C224 H382 K6 N24 O8 Si12
• Title of publication: Insights into the making of a stable silylene.
• Authors of publication: Gehrhus, Barbara; Hitchcock, Peter B.; Pongtavornpinyo, Ruti; Zhang, Lihong
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 15
• Pages of publication: 1847 - 1857
• a: 22.8776 ± 0.0007 Å
• b: 15.9344 ± 0.0006 Å
• c: 33.8306 ± 0.0011 Å
• α: 90°
• β: 101.086 ± 0.002°
• γ: 90°
• Cell volume: 12102.5 ± 0.7 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.1807
• Residual factor for significantly intense reflections: 0.1132
• Weighted residual factors for significantly intense reflections: 0.2164
• Weighted residual factors for all reflections included in the refinement: 0.2495
• Goodness-of-fit parameter for all reflections included in the refinement: 1.056
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No