Information card for entry 7006922

Structure parameters

• Common name: (CPh3)(F-PBB)
• Formula: C55 H15 B F28
• Calculated formula: C55 H15 B F28
• Title of publication: The synthesis of new weakly coordinating diborate anions: anion stability as a function of linker structure and steric bulk.
• Authors of publication: Hannant, Mark H.; Wright, Joseph A.; Lancaster, Simon J.; Hughes, David L.; Horton, Peter N.; Bochmann, Manfred
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 20
• Pages of publication: 2415 - 2426
• a: 9.788 ± 0.002 Å
• b: 18.682 ± 0.004 Å
• c: 27.788 ± 0.006 Å
• α: 90.21 ± 0.03°
• β: 92.34 ± 0.03°
• γ: 104.52 ± 0.03°
• Cell volume: 4914.4 ± 1.9 ų
• Cell temperature: 140 ± 1 K
• Ambient diffraction temperature: 140 ± 1 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2016
• Residual factor for significantly intense reflections: 0.0971
• Weighted residual factors for significantly intense reflections: 0.2163
• Weighted residual factors for all reflections included in the refinement: 0.2567
• Goodness-of-fit parameter for all reflections included in the refinement: 0.887
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No