Information card for entry 7006995

Structure parameters

• Formula: C44 H58 Li2 N4 O4 Si
• Calculated formula: C44 H58 Li2 N4 O4 Si
• SMILES: [Li]1([O]2CCCC2)([O]2CCCC2)N(C(c2ccccc2)=[N]2c3ccccc3)[Si](C)(C)N([Li]2([O]2CCCC2)[O]2CCCC2)C(=[N]1c1ccccc1)c1ccccc1
• Title of publication: A convenient route to silyl linked bis(amidinate) ligands and synthesis of group(I) metal derivatives.
• Authors of publication: Bai, Sheng-Di; Guo, Jian-Ping; Liu, Dian-Sheng
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 18
• Pages of publication: 2244 - 2250
• a: 12.913 ± 0.003 Å
• b: 17.185 ± 0.004 Å
• c: 19.212 ± 0.004 Å
• α: 90°
• β: 96.383 ± 0.003°
• γ: 90°
• Cell volume: 4236.9 ± 1.6 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1059
• Residual factor for significantly intense reflections: 0.0831
• Weighted residual factors for significantly intense reflections: 0.1754
• Weighted residual factors for all reflections included in the refinement: 0.1855
• Goodness-of-fit parameter for all reflections included in the refinement: 1.174
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No