Information card for entry 7007069

Structure parameters

• Formula: C24 H24 N2 O2 P4
• Calculated formula: C24 H24 N2 O2 P4
• SMILES: c12cccc3cccc([P@](=O)(P1P1c4cccc5cccc([P@]1(=O)N(C)C)c45)N(C)C)c23
• Title of publication: Preparation and structures of 1,2-dihydro-1,2-diphosphaacenaphthylenes and rigid backbone stabilized triphosphenium cation.
• Authors of publication: Kilian, Petr; Slawin, Alexandra M. Z.; Woollins, J. Derek
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 18
• Pages of publication: 2175 - 2183
• a: 18.52 ± 0.006 Å
• b: 7.1417 ± 0.0013 Å
• c: 18.136 ± 0.005 Å
• α: 90°
• β: 109.745 ± 0.006°
• γ: 90°
• Cell volume: 2257.7 ± 1 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0698
• Residual factor for significantly intense reflections: 0.048
• Weighted residual factors for significantly intense reflections: 0.1011
• Weighted residual factors for all reflections included in the refinement: 0.1116
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No