Information card for entry 7007092

Structure parameters

• Formula: C51.5 H59.5 N Nb O2 P Si2
• Calculated formula: C51.5 H59.5 N Nb O2 P Si2
• Title of publication: Activation of a CNXylyl ancillary ligand in the reaction of electron-deficient alkynes with a phosphido niobocene complex.
• Authors of publication: Antiñolo, Antonio; García-Yuste, Santiago; Lopez-Solera, Maria Isabel; Otero, Antonio; Pérez-Flores, Juan C; Reguillo-Carmona, Rebeca; Villaseñor, Elena
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 12
• Pages of publication: 1495 - 1496
• a: 10.7939 ± 0.0005 Å
• b: 12.2093 ± 0.0006 Å
• c: 19.3334 ± 0.0009 Å
• α: 93.144 ± 0.003°
• β: 102.049 ± 0.003°
• γ: 108.324 ± 0.003°
• Cell volume: 2345.4 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0771
• Residual factor for significantly intense reflections: 0.0494
• Weighted residual factors for significantly intense reflections: 0.1338
• Weighted residual factors for all reflections included in the refinement: 0.1792
• Goodness-of-fit parameter for all reflections included in the refinement: 0.653
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No