Information card for entry 7007319

Structure parameters

• Formula: C20 H39 Mn3 O35.5 Rh2
• Calculated formula: C20 H18 Mn3 O35.5 Rh2
• Title of publication: Heptacoordinated Mn(II) in oxalate-based bimetallic 2D magnets: synthesis and characterisation of [Mn(L)6][Mn(CH3OH)M(III)(ox)3]2 (M(III) = Cr, Rh; ox = oxalate dianion; L = H2O, CH3OH).
• Authors of publication: Coronado, Eugenio; Galán-Mascarós, José Ramón; Martí-Gastaldo, Carlos; Martínez, Ana Murcia
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 27
• Pages of publication: 3294 - 3299
• a: 9.514 ± 0.0001 Å
• b: 16.072 ± 0.0003 Å
• c: 14.948 ± 0.0002 Å
• α: 90°
• β: 105.356 ± 0.0007°
• γ: 90°
• Cell volume: 2204.08 ± 0.06 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0673
• Residual factor for significantly intense reflections: 0.0486
• Weighted residual factors for significantly intense reflections: 0.13
• Weighted residual factors for all reflections included in the refinement: 0.141
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No