Design, synthesis and photoelectrochemical properties of hexagonal metallomacrocycles based on triphenylamine: [M6(4,4'-bis(2,2':6',2''-terpyridinyl)triphenylamine)6(X)12]; [M = Fe(II), PF6- and Zn(II), BF4-].
Authors of publication
Hwang, Seok-Ho; Moorefield, Charles N.; Wang, Pingshan; Fronczek, Frank R.; Courtney, Brandy H.; Newkome, George R.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2006
Journal issue
29
Pages of publication
3518 - 3522
a
12.9078 ± 0.001 Å
b
13.573 ± 0.002 Å
c
13.602 ± 0.002 Å
α
90.432 ± 0.006°
β
109.097 ± 0.007°
γ
115.196 ± 0.006°
Cell volume
2007.4 ± 0.5 Å3
Cell temperature
110 K
Ambient diffraction temperature
110 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0944
Residual factor for significantly intense reflections
0.0573
Weighted residual factors for significantly intense reflections
0.1377
Weighted residual factors for all reflections included in the refinement
0.1537
Goodness-of-fit parameter for all reflections included in the refinement
