Information card for entry 7007515

Structure parameters

• Common name: catena-((mu!3$-Acetylacetonato-O,O,O',O')-(mu!2$- acetylacetonato-O,O,O')-lead(ii))
• Chemical name: catena-((μ~3~-Acetylacetonato-O,O,O',O')-(μ~2~-acetylacetonato-O,O,O')- lead(II))
• Formula: C10 H14 O4 Pb
• Calculated formula: C10 H14 O4 Pb
• SMILES: [Pb]12([O]=C(C)C=C(C)O1)[O]=C(C)C=C(C)O2
• Title of publication: Crystal structure of lead(II) acetylacetonate and the structure of the acetylacetone solvated lead(II) ion in solution studied by large-angle X-ray scattering.
• Authors of publication: Lyczko, Krzysztof; Narbutt, Jerzy; Paluchowska, Beata; Maurin, Jan K.; Persson, Ingmar
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 33
• Pages of publication: 3972 - 3976
• a: 8.083 ± 0.002 Å
• b: 7.83 ± 0.002 Å
• c: 18.94 ± 0.004 Å
• α: 90°
• β: 94.74 ± 0.03°
• γ: 90°
• Cell volume: 1194.6 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1337
• Residual factor for significantly intense reflections: 0.055
• Weighted residual factors for significantly intense reflections: 0.1416
• Weighted residual factors for all reflections included in the refinement: 0.1723
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No