Information card for entry 7007727

Structure parameters

• Formula: C36 H40 Cl3 N2 Sb
• Calculated formula: C36 H40 Cl3 N2 Sb
• SMILES: C12C(c3cccc4cccc1c34)=[N](c1c(cccc1C(C)C)C(C)C)[Sb](Cl)(Cl)(Cl)[N]=2c1c(cccc1C(C)C)C(C)C
• Title of publication: Complexes of 1,2-bis(aryl-imino)acenaphthene (Ar-BIAN) ligands with some heavy p-block elements.
• Authors of publication: Hill, Nicholas J.; Reeske, Gregor; Moore, Jennifer A.; Cowley, Alan H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2006
• Journal issue: 40
• Pages of publication: 4838 - 4844
• a: 34.4781 ± 0.0006 Å
• b: 10.9074 ± 0.0002 Å
• c: 22.4939 ± 0.0005 Å
• α: 90°
• β: 106.887 ± 0.001°
• γ: 90°
• Cell volume: 8094.4 ± 0.3 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0743
• Residual factor for significantly intense reflections: 0.0484
• Weighted residual factors for significantly intense reflections: 0.1273
• Weighted residual factors for all reflections included in the refinement: 0.1382
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No