Encapsulation of hydride by molecular main group metal clusters: manipulating the source and coordination sphere of the interstitial ion.
Authors of publication
Boss, Sally R.; Coles, Martyn P.; Eyre-Brook, Vicki; García, Felipe; Haigh, Robert; Hitchcock, Peter B.; McPartlin, Mary; Morey, James V.; Naka, Hiroshi; Raithby, Paul R.; Sparkes, Hazel A.; Tate, Christopher W.; Wheatley, Andrew E. H.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2006
Journal issue
47
Pages of publication
5574 - 5582
a
22.756 ± 0.005 Å
b
15.126 ± 0.003 Å
c
16.689 ± 0.003 Å
α
90°
β
94.85 ± 0.03°
γ
90°
Cell volume
5724 ± 2 Å3
Cell temperature
180 ± 2 K
Ambient diffraction temperature
180 ± 2 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.1341
Residual factor for significantly intense reflections
0.1025
Weighted residual factors for significantly intense reflections
0.2812
Weighted residual factors for all reflections included in the refinement
0.3141
Goodness-of-fit parameter for all reflections included in the refinement
