Crystallography Open Database

Information card for entry 7008011

Preview

Coordinates	7008011.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C42 H35 B2 Cl F4 N7 O P Ru
Calculated formula	C42 H35 B2 Cl F4 N7 O P Ru
Title of publication	Regioselective nucleophilic addition of triphenylphosphine to the nitrosylruthenium alkynyl complexes having a hydrotris(pyrazol-1-yl)borate: formation of phosphonio-alkenyl, alkynyl, and allenyl species.
Authors of publication	Nishimura, Yoshimasa; Arikawa, Yasuhiro; Inoue, Takanori; Onishi, Masayoshi
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2005
Journal issue	5
Pages of publication	930 - 937
a	11.1299 ± 0.0005 Å
b	21.586 ± 0.002 Å
c	17.4043 ± 0.0002 Å
α	90°
β	91.2394 ± 0.0003°
γ	90°
Cell volume	4180.4 ± 0.4 Å³
Cell temperature	296.2 K
Number of distinct elements	9
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for significantly intense reflections	0.0415
Weighted residual factors for all reflections included in the refinement	0.0904
Goodness-of-fit parameter for all reflections included in the refinement	1.142
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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