Information card for entry 7008245

Structure parameters

• Common name: (K(tmeda)(C11H8N))n
• Formula: C17 H24 K N3
• Calculated formula: C17 H24 K N3
• Title of publication: Structural studies of group 1 metal 4-azapentalenyl complexes.
• Authors of publication: Bermingham, Michael J.; Cloke, F Geoffrey N; Gardiner, Michael G.; Hitchcock, Peter B.; Wise, Lauren E.; Yates, Brian F.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 7
• Pages of publication: 1157 - 1158
• a: 10.1459 ± 0.0002 Å
• b: 17.4901 ± 0.0004 Å
• c: 20.997 ± 0.0005 Å
• α: 77.087 ± 0.001°
• β: 82.899 ± 0.002°
• γ: 82.008 ± 0.001°
• Cell volume: 3579.91 ± 0.14 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1079
• Residual factor for significantly intense reflections: 0.0881
• Weighted residual factors for significantly intense reflections: 0.222
• Weighted residual factors for all reflections included in the refinement: 0.2407
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No