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Information card for entry 7008288
Preview
Coordinates | 7008288.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C8 H12 F9 N4 Sb Ti |
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Calculated formula | C8 H12 F9 N4 Sb Ti |
SMILES | [Ti](F)(F)(F)([N]#CC)([N]#CC)[N]#CC.[Sb](F)(F)(F)(F)(F)[F-].CC#N |
Title of publication | Hexafluoroantimony(V) salts of the cationic Ti(IV) fluoride non metallocene complexes [TiF3(MeCN)3]+ and [TiF2L]2+ (L = 15-Crown-5 and 18-Crown-6). Preparation, characterization and thermodynamic stability. |
Authors of publication | Decken, Andreas; Ilyin, Evgeny G.; Brooke Jenkins, H. Donald; Nikiforov, Grigori B.; Passmore, Jack |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2005 |
Journal issue | 18 |
Pages of publication | 3039 - 3050 |
a | 8.7491 ± 0.0018 Å |
b | 23.322 ± 0.005 Å |
c | 8.8016 ± 0.0019 Å |
α | 90° |
β | 96.995 ± 0.004° |
γ | 90° |
Cell volume | 1782.6 ± 0.7 Å3 |
Cell temperature | 198 ± 1 K |
Ambient diffraction temperature | 198 ± 1 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0781 |
Residual factor for significantly intense reflections | 0.06 |
Weighted residual factors for significantly intense reflections | 0.1679 |
Weighted residual factors for all reflections included in the refinement | 0.182 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.078 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7008288.html
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