Information card for entry 7008422

Structure parameters

• Formula: C38 H35 N4 Ni3 O18.5
• Calculated formula: C38 H32 N4 Ni3 O18.5
• Title of publication: Three-dimensional mesomeric networks assembled from helix-linked sheets: syntheses, structures, and magnetisms.
• Authors of publication: Qin, Chao; Wang, Xin-Long; Li, Yang-Guang; Wang, En-Bo; Su, Zhong-Min; Xu, Lin; Clérac, Rodolphe
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 15
• Pages of publication: 2609 - 2614
• a: 22.635 ± 0.005 Å
• b: 17.286 ± 0.004 Å
• c: 10.058 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3935.4 ± 1.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0388
• Residual factor for significantly intense reflections: 0.0333
• Weighted residual factors for significantly intense reflections: 0.086
• Weighted residual factors for all reflections included in the refinement: 0.0879
• Goodness-of-fit parameter for all reflections included in the refinement: 0.998
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No