Information card for entry 7008731

Structure parameters

• Formula: C84 H106 Ag4 Cl4 N6 O24 S8
• Calculated formula: C84 H106 Ag4 Cl4 N6 O24 S8
• Title of publication: Donor effect on supramolecular structures of silver(I) perchlorate complexes of macrocycles with O2S2X (X=S, O and NH) donor sets.
• Authors of publication: Yoon, Il; Seo, Joobeom; Lee, Ji-Eun; Song, Mi Ryoung; Lee, So Young; Choi, Kyu Seong; Jung, Ok-Sang; Park, Ki-Min; Lee, Shim Sung
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 14
• Pages of publication: 2352 - 2354
• a: 11.5691 ± 0.0008 Å
• b: 13.3821 ± 0.001 Å
• c: 16.2842 ± 0.0012 Å
• α: 85.787 ± 0.001°
• β: 75.283 ± 0.001°
• γ: 82.898 ± 0.001°
• Cell volume: 2417.4 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0739
• Residual factor for significantly intense reflections: 0.0444
• Weighted residual factors for significantly intense reflections: 0.1111
• Weighted residual factors for all reflections included in the refinement: 0.1282
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No