Information card for entry 7008786

Structure parameters

• Formula: C38 H71 Cl2 N7 Ni2 P2 S4
• Calculated formula: C38 H71 Cl2 N7 Ni2 P2 S4
• Title of publication: Bis(isothiocyanato)bis(phosphine) complexes of group 10 metals: reactivity toward organic isocyanides
• Authors of publication: Chang, Xiaohong; Lee, Kyung-Eun; Il Jeon, Sang; Kim, Yong-Joo; Lee, H.-K.; Lee, Soon W.
• Journal of publication: Dalton Transactions
• Year of publication: 2005
• Journal issue: 23
• Pages of publication: 3722
• a: 13.104 ± 0.004 Å
• b: 13.141 ± 0.004 Å
• c: 17.539 ± 0.003 Å
• α: 81.16 ± 0.019°
• β: 82.24 ± 0.02°
• γ: 67.39 ± 0.02°
• Cell volume: 2745.4 ± 1.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1797
• Residual factor for significantly intense reflections: 0.094
• Weighted residual factors for significantly intense reflections: 0.2354
• Weighted residual factors for all reflections included in the refinement: 0.2974
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No