Crystallography Open Database

Information card for entry 7008859

Preview

Coordinates	7008859.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	Rh2(OAc)4[(OAc)(H2hpp)]2, 3CH2Cl2
Formula	C29 H52 Cl6 N6 O12 Rh2
Calculated formula	C29 H52 Cl6 N6 O12 Rh2
Title of publication	A hardwon dirhodium paddlewheel with guanidinate type (hpp) bridging ligands
Authors of publication	Berry, John F.; Cotton, F. Albert; Huang, Penglin; Murillo, Carlos A.; Wang, Xiaoping
Journal of publication	Dalton Transactions
Year of publication	2005
Journal issue	23
Pages of publication	3713
a	17.368 ± 0.008 Å
b	14.227 ± 0.006 Å
c	20.933 ± 0.009 Å
α	90°
β	107.792 ± 0.007°
γ	90°
Cell volume	4925 ± 4 Å³
Cell temperature	213 ± 2 K
Ambient diffraction temperature	213 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0807
Residual factor for significantly intense reflections	0.0669
Weighted residual factors for significantly intense reflections	0.1901
Weighted residual factors for all reflections included in the refinement	0.2021
Goodness-of-fit parameter for all reflections included in the refinement	1.079
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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