Information card for entry 7008890

Structure parameters

• Formula: C13 H25 Cl2 N3.5 Ni O9 S2
• Calculated formula: C12.5 H25 Cl2 N3.25 Ni O9 S2
• Title of publication: Nickel(II) complexes with dithiadiiminoamine and dithiabis(thiosemicarbazone) ligands †
• Authors of publication: Pavlishchuk, Vitaly V.; Kolotilov, Sergey V.; Addison, Anthony W.; Butcher, Raymond J.; Sinn, Ekkehard
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 3
• Pages of publication: 335
• a: 22.046 ± 0.009 Å
• b: 11.339 ± 0.004 Å
• c: 21.319 ± 0.009 Å
• α: 90°
• β: 117.363 ± 0.002°
• γ: 90°
• Cell volume: 4733 ± 3 ų
• Cell temperature: 291.2 K
• Ambient diffraction temperature: 291.2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for significantly intense reflections: 0.0924
• Weighted residual factors for all reflections included in the refinement: 0.065
• Goodness-of-fit parameter for all reflections included in the refinement: 2.237
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No