Information card for entry 7009008

Structure parameters

• Formula: C44 H35 F3 N2 O2 P2 Pd
• Calculated formula: C44 H35 F3 N2 O2 P2 Pd
• Title of publication: Synthesis and chemistry of diphenyl-2-pyridylphosphine complexes of palladium(0). X-Ray characterisation of Pd(Ph2Ppy)2(η2-DMAD) and trans-Pd(Ph2Ppy)2(PhCCH2)(CF3CO2)
• Authors of publication: Dervisi, Athanasia; Edwards, Peter G.; Newman, Paul D.; Tooze, Robert P.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 4
• Pages of publication: 523
• a: 11.837 ± 0.002 Å
• b: 13.342 ± 0.007 Å
• c: 13.729 ± 0.003 Å
• α: 95.32 ± 0.07°
• β: 103.28 ± 0.02°
• γ: 110.28 ± 0.03°
• Cell volume: 1943.8 ± 1.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.112
• Residual factor for significantly intense reflections: 0.0397
• Weighted residual factors for all reflections: 0.074
• Weighted residual factors for significantly intense reflections: 0.0587
• Goodness-of-fit parameter for all reflections: 0.437
• Goodness-of-fit parameter for significantly intense reflections: 0.645
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No