Information card for entry 7009037

Structure parameters

• Chemical name: Tetrabromodi(μ-bisdiphenylstibinomethane)dipalladium(II).2dichloromethane
• Formula: C52 H48 Br4 Cl4 Pd2 Sb4
• Calculated formula: C51.072 Br4 Cl2.144 Pd2 Sb4
• Title of publication: Synthesis, properties and structures of complexes of platinum metal halides and Group 11 metals with two distibinomethane ligands, R2SbCH2SbR2 (R = Me or Ph)
• Authors of publication: Even, Tina; Genge, Anthony R. J.; Hill, Angela M.; Holmes, Nicholas J.; Levason, William; Webster, Michael
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 5
• Pages of publication: 655
• a: 15.953 ± 0.005 Å
• b: 17 ± 0.004 Å
• c: 11.943 ± 0.003 Å
• α: 109.18 ± 0.02°
• β: 109.95 ± 0.02°
• γ: 79.65 ± 0.02°
• Cell volume: 2867.2 ± 1.4 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0651
• Residual factor for significantly intense reflections: 0.0651
• Weighted residual factors for all reflections: 0.0762
• Weighted residual factors for all reflections included in the refinement: 0.0762
• Goodness-of-fit parameter for all reflections: 2.469
• Goodness-of-fit parameter for all reflections included in the refinement: 2.469
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No