Information card for entry 7009075

Structure parameters

• Formula: C27 H43 Cl2 N8 O0.5 Pd
• Calculated formula: C27 H42.5 Cl2 N8 O0.5 Pd
• Title of publication: Palladium(II) chloride complexes with 1,2,4-triazolo[1,5-a]pyrimidines: X-ray, 15N‒1H NMR and 15N CP MAS studies
• Authors of publication: Szłyk, Edward; Grodzicki, Antoni; Pazderski, Leszek; Wojtczak, Andrzej; Chatłas, Janusz; Wrzeszcz, Grzegorz; Sitkowski, Jerzy; Kamieński, Bohdan
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 6
• Pages of publication: 867
• a: 10.743 ± 0.0006 Å
• b: 11.0134 ± 0.0005 Å
• c: 14.134 ± 0.0006 Å
• α: 75.342 ± 0.004°
• β: 81.431 ± 0.004°
• γ: 79.665 ± 0.004°
• Cell volume: 1582.16 ± 0.14 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0583
• Residual factor for significantly intense reflections: 0.0403
• Weighted residual factors for significantly intense reflections: 0.098
• Weighted residual factors for all reflections included in the refinement: 0.1082
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No