Information card for entry 7009130

Structure parameters

• Formula: C63 H74 Cl2 N O3 P4 Pd3 S4
• Calculated formula: C63 H66 Cl2 N O3 P4 Pd3 S4
• Title of publication: A new access to palladium‒phosphine chemistry. Formation of polynuclear palladium compounds via the oxidation of ligands in simple palladium(II) complexes
• Authors of publication: Su, Weiping; Cao, Rong; Hong, Maochun; Wu, Daxu; Lu, Jiaxi
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 9
• Pages of publication: 1527
• a: 27.118 ± 0.005 Å
• b: 14.987 ± 0.003 Å
• c: 20.477 ± 0.004 Å
• α: 90°
• β: 126.65 ± 0.03°
• γ: 90°
• Cell volume: 6677 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1466
• Residual factor for significantly intense reflections: 0.0678
• Weighted residual factors for all reflections: 0.1634
• Weighted residual factors for significantly intense reflections: 0.1277
• Goodness-of-fit parameter for all reflections: 1.044
• Goodness-of-fit parameter for significantly intense reflections: 1.152
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No