Crystallography Open Database

Information card for entry 7009147

Preview

Coordinates	7009147.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C94 H112 Cl24 O8 P2 Pd2
Calculated formula	C94 H112 Cl24 O8 P2 Pd2
Title of publication	Calix[4]arene derived phosphites: their hydrolytic stability and complexes with gold(I), platinum(II,0), palladium(II) and iridium(I)
Authors of publication	Cobley, Christopher J.; Ellis, Dianne D.; Orpen, A. Guy; Pringle, Paul G.
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2000
Journal issue	7
Pages of publication	1101
a	13.312 ± 0.003 Å
b	13.923 ± 0.003 Å
c	16.352 ± 0.003 Å
α	106.68 ± 0.03°
β	95.68 ± 0.03°
γ	107.47 ± 0.03°
Cell volume	2711.9 ± 1.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0758
Residual factor for significantly intense reflections	0.0507
Weighted residual factors for all reflections	0.1482
Weighted residual factors for significantly intense reflections	0.126
Goodness-of-fit parameter for all reflections	1.09
Goodness-of-fit parameter for significantly intense reflections	1.09
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7009147.html