Information card for entry 7009150

Structure parameters

• Formula: C58.75 H78 Cl3 O7 P Rh
• Calculated formula: C58.75 H75 Cl3 O7 P Rh
• Title of publication: Rhodium(I) complexes of robust phosphites derived from calix[4]arenes and their application in the hydroformylation of 1-hexene
• Authors of publication: Cobley, Christopher J.; Ellis, Dianne D.; Orpen, A. Guy; Pringle, Paul G.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 7
• Pages of publication: 1109
• a: 15.276 ± 0.002 Å
• b: 18.109 ± 0.003 Å
• c: 21.303 ± 0.003 Å
• α: 94.378 ± 0.01°
• β: 93.617 ± 0.01°
• γ: 96.183 ± 0.013°
• Cell volume: 5826.6 ± 1.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0869
• Residual factor for significantly intense reflections: 0.0621
• Weighted residual factors for all reflections: 0.1612
• Weighted residual factors for significantly intense reflections: 0.1352
• Goodness-of-fit parameter for all reflections: 1.113
• Goodness-of-fit parameter for significantly intense reflections: 1.121
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No