Information card for entry 7009215

Structure parameters

• Formula: C27 H45 N6 Sb Si3
• Calculated formula: C27 H45 N6 Sb Si3
• Title of publication: Geminal arsa(III)amide and trisubstituted antimony and bismuth amides from the sterically hindered, N-functionalised amido ligand [{2-(6-Me)C5H3N}NSiMe3]−
• Authors of publication: Raston, Colin L.; Skelton, Brian W.; Tolhurst, Vicki-Anne; White, Allan H.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 8
• Pages of publication: 1279
• a: 14.865 ± 0.006 Å
• b: 11.682 ± 0.017 Å
• c: 11.296 ± 0.01 Å
• α: 116.13 ± 0.09°
• β: 94.04 ± 0.05°
• γ: 104.01 ± 0.07°
• Cell volume: 1673 ± 3 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.028
• Residual factor for significantly intense reflections: 0.025
• Weighted residual factors for all reflections: 0.032
• Weighted residual factors for all reflections included in the refinement: 0.032
• Goodness-of-fit parameter for all reflections: 1.378
• Goodness-of-fit parameter for all reflections included in the refinement: 1.458
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No