Information card for entry 7009241

Structure parameters

• Chemical name: 1,1-Bis(N,N-dimethylaminoxy)-2,3,4,5-tetraphenyl-1-germacyclopentadien
• Formula: C32 H32 Ge N2 O2
• Calculated formula: C32 H32 Ge N2 O2
• SMILES: [Ge]1(ON(C)C)(ON(C)C)C(=C(c2ccccc2)C(=C1c1ccccc1)c1ccccc1)c1ccccc1
• Title of publication: Siloles and germoles modified by partial hypercoordination through aminoxy substituents
• Authors of publication: Losehand, Udo; Mitzel, Norbert W.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 7
• Pages of publication: 1049
• a: 12.399 ± 0.004 Å
• b: 12.453 ± 0.003 Å
• c: 19.955 ± 0.003 Å
• α: 81.16 ± 0.02°
• β: 84.37 ± 0.02°
• γ: 66.05 ± 0.02°
• Cell volume: 2780.2 ± 1.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2201
• Residual factor for significantly intense reflections: 0.0659
• Weighted residual factors for significantly intense reflections: 0.1401
• Weighted residual factors for all reflections included in the refinement: 0.1825
• Goodness-of-fit parameter for all reflections included in the refinement: 0.998
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No