Information card for entry 7009253

Structure parameters

• Common name: compound 7c(Mn)
• Formula: C34 H54 Co2 Mn2 N2 O24 P6
• Calculated formula: C34 H54 Co2 Mn2 N2 O24 P6
• Title of publication: An entry to half-sandwich complexes of first row transition metals (Ni, Co, Mn) containing the Kläui tripodal ligand, LOMe: synthesis and crystal structures of oligomeric, [LOMeM(μ-X)(L)]n (n = 2, 4), and monomeric complexes, LOMeM(L2)(X)
• Authors of publication: De-qiang Ma; Shiro Hikichi; Munetaka Akita; Yoshihiko Moro-oka
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2000
• Journal issue: 7
• Pages of publication: 1123 - 1134
• a: 15.558 ± 0.008 Å
• b: 19.023 ± 0.007 Å
• c: 8.898 ± 0.003 Å
• α: 97.65 ± 0.02°
• β: 92.1 ± 0.03°
• γ: 80.74 ± 0.03°
• Cell volume: 2575.7 ± 1.9 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1538
• Residual factor for significantly intense reflections: 0.1332
• Weighted residual factors for significantly intense reflections: 0.3107
• Weighted residual factors for all reflections included in the refinement: 0.3215
• Goodness-of-fit parameter for all reflections included in the refinement: 2.067
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No