Information card for entry 7009290

Structure parameters

• Formula: C34 H26 Mn N8
• Calculated formula: C34 H26 Mn N8
• SMILES: [Mn]1234([N](=Nc5[n]2cccc5)c2ccccc2N3c2ccccc2)[N](=Nc2[n]1cccc2)c1ccccc1N4c1ccccc1
• Title of publication: Low-spin manganese(II) and cobalt(III) complexes of N-aryl-2-pyridylazophenylamines: new tridentate N,N,N-donors derived from cobalt mediated aromatic ring amination of 2-(phenylazo)pyridine. Crystal structure of a manganese(II) complex †
• Authors of publication: Saha, Amrita; Majumdar, Partha; Goswami, Sreebrata
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 11
• Pages of publication: 1703
• a: 10.3746 ± 0.0017 Å
• b: 16.061 ± 0.006 Å
• c: 16.726 ± 0.006 Å
• α: 90°
• β: 90.15 ± 0.02°
• γ: 90°
• Cell volume: 2787 ± 1.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0532
• Residual factor for significantly intense reflections: 0.0332
• Weighted residual factors for significantly intense reflections: 0.074
• Weighted residual factors for all reflections included in the refinement: 0.0864
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No