Information card for entry 7009302

Structure parameters

• Chemical name: Triethylammonium-bis{[N,N-bis(2-oxyphenyl)glycinate] oxovanadium(IV)} dichloromethane solvate
• Formula: C48 H68 Cl8 N4 O10 V2
• Calculated formula: C48 H64 Cl8 N4 O10 V2
• Title of publication: Magneto-structural correlation for binuclear octahedral vanadium(IV)–oxo complexes. Synthesis, structure and magnetic properties of a VIVO2+ complex with a new ligand derived from glycine
• Authors of publication: Ceccato, Augusto S.; Neves, Ademir; de Brito, Marcos A.; Drechsel, Sueli M.; Mangrich, Antonio S.; Werner, Rüdiger; Haase, Wolfgang; Bortoluzzi, Adailton J.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 10
• Pages of publication: 1573
• a: 10.638 ± 0.002 Å
• b: 11.38 ± 0.002 Å
• c: 13.512 ± 0.002 Å
• α: 98.11 ± 0.03°
• β: 102 ± 0.03°
• γ: 110.17 ± 0.03°
• Cell volume: 1461 ± 0.6 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0476
• Residual factor for significantly intense reflections: 0.0406
• Weighted residual factors for significantly intense reflections: 0.1105
• Weighted residual factors for all reflections included in the refinement: 0.1149
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No