Information card for entry 7009318

Structure parameters

• Formula: C34 H22 N2 O8 Os3 P
• Calculated formula: C34 H22 N2 O8 Os3 P
• SMILES: [Os]12([Os]([Os]3(C#[O])(C#[O])C#[O])(C#[O])(C#[O])(C#[O])C(c4[n]3cccc4)C[N]1=Cc1c([P]2(c2ccccc2)c2ccccc2)cccc1)(C#[O])C#[O]
• Title of publication: Complexation and metallation of the multifunctional [Ph2P(o-C6H4)CHN(CH2)2(o-C5H4N)] ligand on triosmium carbonyl clusters
• Authors of publication: Yeh, Wen-Yann; Yang, Ching-Chao; Peng, Shie-Ming; Lee, Gene-Hsiang
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 10
• Pages of publication: 1649
• a: 10.0659 ± 0.0001 Å
• b: 13.4957 ± 0.0001 Å
• c: 13.6217 ± 0.0001 Å
• α: 66.709 ± 0.001°
• β: 84.669 ± 0.001°
• γ: 85.686 ± 0.001°
• Cell volume: 1690.81 ± 0.03 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0535
• Residual factor for significantly intense reflections: 0.0313
• Weighted residual factors for all reflections: 0.0591
• Weighted residual factors for significantly intense reflections: 0.0544
• Goodness-of-fit parameter for all reflections: 1.003
• Goodness-of-fit parameter for significantly intense reflections: 1.079
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No