Information card for entry 7009399

Structure parameters

• Formula: C30 H54 K O6 P
• Calculated formula: C30 H53 K O6 P
• Title of publication: Synthesis and crystal structure determination of two monomeric alkali metal phosphide derivatives: [M{P(H)C6H2-t-Bu3-2,4,6}(18-crown-6)] (M = K or Rb)
• Authors of publication: Rabe, Gerd W.; Heise, Henrike; Liable-Sands, Louise M.; Guzei, Ilia A.; Rheingold, Arnold L.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 12
• Pages of publication: 1863
• a: 40.7745 ± 0.0002 Å
• b: 9.0007 ± 0.0002 Å
• c: 19.1484 ± 0.0003 Å
• α: 90°
• β: 106.655 ± 0.001°
• γ: 90°
• Cell volume: 6732.63 ± 0.19 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0881
• Residual factor for significantly intense reflections: 0.0572
• Weighted residual factors for all reflections: 0.1809
• Weighted residual factors for significantly intense reflections: 0.1509
• Goodness-of-fit parameter for all reflections: 1.146
• Goodness-of-fit parameter for significantly intense reflections: 1.23
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No