Information card for entry 7009411

Structure parameters

• Formula: C24 H39 Li N4
• Calculated formula: C24 H39 Li N4
• SMILES: N([C@H](C)c1ccccc1)(Cc1ccccc1)[Li]12[N](CC[N]2(CC[N]1(C)C)C)(C)C
• Title of publication: Solid state structures of the chiral lithium amide complexes (S )-[(Ph(Me)CH)(PhCH2)NLi·thf]2 and (R)-[(Ph(Me)CH)(PhCH2)NLi·pmdta] †
• Authors of publication: Andrews, Philip C.; Duggan, Peter J.; Fallon, Gary D.; McCarthy, Tom D.; Peatt, Anna C.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 12
• Pages of publication: 1937
• a: 9.0295 ± 0.0002 Å
• b: 12.6622 ± 0.0004 Å
• c: 10.534 ± 0.0003 Å
• α: 90°
• β: 96.161 ± 0.002°
• γ: 90°
• Cell volume: 1197.43 ± 0.06 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 4
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0964
• Residual factor for significantly intense reflections: 0.0776
• Weighted residual factors for significantly intense reflections: 0.1734
• Weighted residual factors for all reflections included in the refinement: 0.1877
• Goodness-of-fit parameter for all reflections included in the refinement: 1.089
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No