Information card for entry 7009417

Structure parameters

• Formula: C72 H114 K2 N8 Ni2 O18 P2
• Calculated formula: C72 H112 K2 N8 Ni2 O18 P2
• Title of publication: Two new bimetallic phosphido carbonyl complexes of nickel(0): [Ni2(CO)2(PPh3)2(μ-CO)(μ-PPh2)]− and [Ni2(CO)4(μ-PPh2)2]2−
• Authors of publication: Keşanlı, Banu; Gardner, Donna Rae; Scott, Brian; Eichhorn, Bryan W.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 8
• Pages of publication: 1291
• a: 11.211 ± 0.004 Å
• b: 13.861 ± 0.002 Å
• c: 13.942 ± 0.002 Å
• α: 76.55°
• β: 82.76°
• γ: 80.78°
• Cell volume: 2071 ± 0.9 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0781
• Residual factor for significantly intense reflections: 0.0691
• Weighted residual factors for all reflections: 0.1778
• Weighted residual factors for significantly intense reflections: 0.1735
• Goodness-of-fit parameter for all reflections: 1.257
• Goodness-of-fit parameter for significantly intense reflections: 1.313
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No