Information card for entry 7009466

Structure parameters

• Formula: C65 H55 Cl4 N2 O P3 Pd2
• Calculated formula: C65 H55 Cl4 N2 O P3 Pd2
• Title of publication: Reactivity of chiral diiminodiphosphine ligands towards PdCl2(PhCN)2: synthesis and crystal structures of two unexpected dinuclear palladium(II) complexes
• Authors of publication: Wong, Wai-Kwok; Zhang, Li-Lu; Chen, Yang; Wong, Wai-Yeung; Wong, Wing-Tak; Xue, Feng; Mak, Thomas C. W.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 9
• Pages of publication: 1397
• a: 12.574 ± 0.001 Å
• b: 13.636 ± 0.001 Å
• c: 20.058 ± 0.001 Å
• α: 80.03 ± 0.01°
• β: 75.67 ± 0.01°
• γ: 81.04 ± 0.01°
• Cell volume: 3258.8 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0722
• Residual factor for significantly intense reflections: 0.0611
• Weighted residual factors for significantly intense reflections: 0.1642
• Weighted residual factors for all reflections included in the refinement: 0.1741
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No