Information card for entry 7009500

Structure parameters

• Chemical name: Trans-1,4bis(diphenylphosphine)-4-methylpyridinetrichlororuthenium(III)
• Formula: C34.5 H35.5 Cl4 N P2 Ru
• Calculated formula: C34.5 H35 Cl4.004 N P2 Ru
• Title of publication: Electrosynthesis of binuclear ruthenium complexes from [RuCl3(dppb)(L)] precursors [L = pyridine, 4-methylpyridine or dimethyl sulfoxide; dppb = 1,4-bis(diphenylphosphino)butane]
• Authors of publication: Wohnrath, Karen; de Araujo, Márcio Peres; Dinelli, Luis Rogério; Batista, Alzir Azevedo; de Sousa Moreira, Icaro; Castellano, Eduardo Ernesto; Ellena, Javier
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 19
• Pages of publication: 3383
• a: 14.785 ± 0.01 Å
• b: 17.559 ± 0.005 Å
• c: 27.448 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7126 ± 5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.2352
• Residual factor for significantly intense reflections: 0.0565
• Weighted residual factors for all reflections: 0.1589
• Weighted residual factors for significantly intense reflections: 0.1228
• Goodness-of-fit parameter for all reflections: 1.189
• Goodness-of-fit parameter for significantly intense reflections: 1.619
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No