Information card for entry 7009547

Structure parameters

• Formula: C74.5 H59 B4 F16 N13 Ni2 O3.5
• Calculated formula: C74.5 H57 B4 F16 N13 Ni2 O3.5
• Title of publication: Self-assembled dinuclear molecular box [Ag2L2]2+ and triple helicates [Co2L3]4+, [Ni2L3]4+{L = bis[4-(2-pyridylmethyleneamino)phenyl] ether}
• Authors of publication: He Cheng; Duan Chun-ying; Fang Chen-jie; Meng Qing-jin
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2000
• Journal issue: 14
• Pages of publication: 2419 - 2424
• a: 22.723 ± 0.008 Å
• b: 18.472 ± 0.006 Å
• c: 20.184 ± 0.009 Å
• α: 90°
• β: 112.71 ± 0.04°
• γ: 90°
• Cell volume: 7815 ± 6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.1892
• Residual factor for significantly intense reflections: 0.0745
• Weighted residual factors for significantly intense reflections: 0.1426
• Weighted residual factors for all reflections included in the refinement: 0.182
• Goodness-of-fit parameter for all reflections included in the refinement: 0.993
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No