Information card for entry 7009569

Structure parameters

• Formula: C62 H60 N9 Ru
• Calculated formula: C62 H60 N9 Ru
• Title of publication: Guanidinates as chelating anionic ligands for early, middle and late transition metals: syntheses and crystal structures of [Ti{η2-(NPh)2CNEt2}2Cl2], [Ru{η2-(NPh)2CNHPh}3] and [Pt{η2-(NPh)2CNHPh}2]
• Authors of publication: Bailey, Philip J.; Grant, Keith J.; Mitchell, Lindsey A.; Pace, Stuart; Parkin, Andrew; Parsons, Simon
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 12
• Pages of publication: 1887
• a: 22.248 ± 0.003 Å
• b: 20.648 ± 0.004 Å
• c: 11.784 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5413.3 ± 1.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0824
• Residual factor for significantly intense reflections: 0.0544
• Weighted residual factors for all reflections: 0.1358
• Weighted residual factors for significantly intense reflections: 0.1096
• Goodness-of-fit parameter for all reflections: 1.043
• Goodness-of-fit parameter for significantly intense reflections: 1.034
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No