Information card for entry 7009651

Structure parameters

• Common name: [KPPh2].1/14(toluene)
• Formula: C12.5 H10.57 K P
• Calculated formula: C12.4286 H10 K P
• Title of publication: Crowded organometallic compounds of the alkali metals with diphenylphosphino substituents in the organic group
• Authors of publication: Avent, Anthony G.; Bonafoux, Dominique; Eaborn, Colin; Hill, Michael S.; Hitchcock, Peter B.; Smith, J. David
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 13
• Pages of publication: 2183
• a: 15.1313 ± 0.0002 Å
• b: 13.7513 ± 0.0002 Å
• c: 39.8676 ± 0.0006 Å
• α: 90°
• β: 94.851 ± 0.001°
• γ: 90°
• Cell volume: 8265.7 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0941
• Residual factor for significantly intense reflections: 0.0546
• Weighted residual factors for significantly intense reflections: 0.1401
• Weighted residual factors for all reflections included in the refinement: 0.1626
• Goodness-of-fit parameter for all reflections included in the refinement: 0.981
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No