Information card for entry 7009656

Structure parameters

• Common name: [Li(tmeda)2][(tsi)Al(StBu)3].2.5(benzene)
• Formula: C49 H101 Al Li N4 S3 Si3
• Calculated formula: C49 H101 Al Li N4 S3 Si3
• Title of publication: Syntheses and crystal structures of some lithium di- and tri-(thiolato)[tris(trimethylsilyl)methyl]aluminates
• Authors of publication: Chen, Wu-Yong; Eaborn, Colin; Gorrell, Ian B.; Hitchcock, Peter B.; Smith, J. David
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 14
• Pages of publication: 2313
• a: 34.256 ± 0.007 Å
• b: 11.863 ± 0.003 Å
• c: 30.519 ± 0.004 Å
• α: 90°
• β: 99.88 ± 0.02°
• γ: 90°
• Cell volume: 12218 ± 4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1906
• Residual factor for significantly intense reflections: 0.086
• Weighted residual factors for significantly intense reflections: 0.166
• Weighted residual factors for all reflections included in the refinement: 0.2114
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No