Synthesis and characterisation of pendant-arm amino derivatives of 1,4,7-triazacyclononane and alkyl-bridged bis(1,4,7-triazacyclononane) macrocycles and complexation to Cu(II)
Authors of publication
Blake, Alexander J.; Danks, Jonathan P.; Li, Wan-Sheung; Lippolis, Vito; Schröder, Martin
Journal of publication
Journal of the Chemical Society, Dalton Transactions
Year of publication
2000
Journal issue
17
Pages of publication
3034
a
11.786 ± 0.002 Å
b
12.189 ± 0.002 Å
c
12.849 ± 0.002 Å
α
107.22 ± 0.01°
β
90.88 ± 0.02°
γ
118.53 ± 0.01°
Cell volume
1521.8 ± 0.5 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0482
Residual factor for significantly intense reflections
0.0417
Weighted residual factors for significantly intense reflections
0.104
Weighted residual factors for all reflections included in the refinement
0.1108
Goodness-of-fit parameter for all reflections included in the refinement
