Information card for entry 7009709

Structure parameters

• Formula: C29 H55 Cl2 Co N6 O11 P
• Calculated formula: C29 H55 Cl2.004 Co N6 O11 P
• Title of publication: Synthesis and molecular structures of a pair of tris(imidazolyl)phosphine cobalt‒perchlorate complexes, {[PimPri2]Co(OClO3)}[ClO4] and {[PimPri2]Co(OH2)(HOMe)(OClO3)}[ClO4]
• Authors of publication: Kimblin, Clare; Bridgewater, Brian M.; Churchill, David G.; Parkin, Gerard
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 13
• Pages of publication: 2191
• a: 12.6185 ± 0.0008 Å
• b: 18.2452 ± 0.0011 Å
• c: 17.6528 ± 0.001 Å
• α: 90°
• β: 90.537 ± 0.001°
• γ: 90°
• Cell volume: 4064 ± 0.4 ų
• Cell temperature: 233 ± 2 K
• Ambient diffraction temperature: 233 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0583
• Residual factor for significantly intense reflections: 0.046
• Weighted residual factors for significantly intense reflections: 0.1222
• Weighted residual factors for all reflections included in the refinement: 0.1294
• Goodness-of-fit parameter for all reflections included in the refinement: 1.094
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No