Information card for entry 7009721

Structure parameters

• Formula: C25 H22 Cl2 Co N5 O9
• Calculated formula: C25 H22 Cl2 Co N5 O9
• Title of publication: The photodecarboxylation of [N,N-bis(2-pyridylmethyl)amino acidato]phenanthrolinecobalt(III) complexes: ‒ formation and decomposition of metallacyclic species †
• Authors of publication: Hartshorn, Richard M.; Telfer, Shane G.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 16
• Pages of publication: 2801
• a: 18.158 ± 0.005 Å
• b: 8.978 ± 0.002 Å
• c: 34.173 ± 0.009 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5571 ± 2 ų
• Cell temperature: 159 ± 2 K
• Ambient diffraction temperature: 159 ± 2 K
• Number of distinct elements: 6
• Space group number: 29
• Hermann-Mauguin space group symbol: P c a 21
• Hall space group symbol: P 2c -2ac
• Residual factor for all reflections: 0.0763
• Residual factor for significantly intense reflections: 0.0431
• Weighted residual factors for significantly intense reflections: 0.1006
• Weighted residual factors for all reflections included in the refinement: 0.1077
• Goodness-of-fit parameter for all reflections included in the refinement: 0.882
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No