Information card for entry 7009823

Structure parameters

• Formula: C49 H42 Cl2 N2 O2 Os P4 S4
• Calculated formula: C49 H42 Cl2 N2 O2 Os P4 S4
• Title of publication: Dioxo- and nitrido-osmium complexes with imidodiphosphinochalcogenido ligands [N(QPR2)2]− (Q = S or Se; R = Ph or Pri)
• Authors of publication: Zhang, Qian-Feng; Lau, Kwok-Kin; Chim, Joyce L. C.; Wong, Terry K. T.; Wong, Wing-Tak; Williams, Ian D.; Leung, Wa-Hung
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 17
• Pages of publication: 3027
• a: 13.289 ± 0.001 Å
• b: 21.226 ± 0.002 Å
• c: 18.002 ± 0.002 Å
• α: 90°
• β: 101.5 ± 0.02°
• γ: 90°
• Cell volume: 4975.9 ± 0.9 ų
• Cell temperature: 298.2 K
• Ambient diffraction temperature: 298.2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor for significantly intense reflections: 0.0291
• Weighted residual factors for significantly intense reflections: 0.0363
• Goodness-of-fit parameter for significantly intense reflections: 2.155
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No