Information card for entry 7009825

Structure parameters

• Formula: C72 H60 N3 Os P6 S6
• Calculated formula: C72 H60 N3 Os P6 S6
• Title of publication: Dioxo- and nitrido-osmium complexes with imidodiphosphinochalcogenido ligands [N(QPR2)2]− (Q = S or Se; R = Ph or Pri)
• Authors of publication: Zhang, Qian-Feng; Lau, Kwok-Kin; Chim, Joyce L. C.; Wong, Terry K. T.; Wong, Wing-Tak; Williams, Ian D.; Leung, Wa-Hung
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 17
• Pages of publication: 3027
• a: 10.953 ± 0.002 Å
• b: 14.611 ± 0.002 Å
• c: 22.038 ± 0.002 Å
• α: 82.64 ± 0.01°
• β: 86.66 ± 0.01°
• γ: 78.73 ± 0.01°
• Cell volume: 3428.3 ± 0.9 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0539
• Residual factor for significantly intense reflections: 0.0378
• Weighted residual factors for significantly intense reflections: 0.0838
• Weighted residual factors for all reflections included in the refinement: 0.0914
• Goodness-of-fit parameter for all reflections included in the refinement: 0.99
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No