Information card for entry 7009835

Structure parameters

• Formula: C23.333 H36 As4 Cl2 Co F6 O0.666 P
• Calculated formula: C23.3323 H32 As4 Cl2 Co F6 O0.666333 P
• Title of publication: Synthesis of chiral multidentate tertiary arsines with As4 or As6 donor atoms
• Authors of publication: Doyle, Roy J.; Habermehl, Nicole; Salem, Geoffrey; Willis, Anthony C.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 20
• Pages of publication: 3603
• a: 21.231 ± 0.002 Å
• b: 21.231 ± 0.002 Å
• c: 18.627 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 7271.3 ± 1.5 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 8
• Space group number: 146
• Hermann-Mauguin space group symbol: R 3 :H
• Hall space group symbol: R 3
• Residual factor for all reflections: 0.043
• Residual factor for significantly intense reflections: 0.035
• Weighted residual factors for all reflections: 0.04
• Weighted residual factors for all reflections included in the refinement: 0.036
• Goodness-of-fit parameter for all reflections: 1.332
• Goodness-of-fit parameter for all reflections included in the refinement: 1.288
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No