Information card for entry 7009837

Structure parameters

• Formula: C35 H54.62 As6 Co F18 O1.31 P3
• Calculated formula: C35 H54 As6 Co F18 O1.31 P3
• Title of publication: Synthesis of chiral multidentate tertiary arsines with As4 or As6 donor atoms
• Authors of publication: Doyle, Roy J.; Habermehl, Nicole; Salem, Geoffrey; Willis, Anthony C.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 20
• Pages of publication: 3603
• a: 13.08 ± 0.003 Å
• b: 24.057 ± 0.004 Å
• c: 31.3 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9849 ± 3 ų
• Cell temperature: 193.2 K
• Ambient diffraction temperature: 193.2 K
• Number of distinct elements: 7
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0768
• Residual factor for significantly intense reflections: 0.0473
• Weighted residual factors for all reflections: 0.0574
• Weighted residual factors for all reflections included in the refinement: 0.0542
• Goodness-of-fit parameter for all reflections: 1.908
• Goodness-of-fit parameter for all reflections included in the refinement: 2.133
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No