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Information card for entry 7009929
Preview
Coordinates | 7009929.cif |
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Original paper (by DOI) | HTML |
Formula | C22 H27 Ir O8 Se2 |
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Calculated formula | C22 H27 Ir O8 Se2 |
Title of publication | Syntheses of diiridium complexes with two bridging tetrachalcogenide ligands [{Ir(η5-C5Me5)}2(μ-E4)2] (E = Se or S) and their reactions with alkynes forming mono- or di-nuclear dichalcogenolene complexes |
Authors of publication | Nagao, Shoken; Seino, Hidetake; Okada, Tomohiko; Mizobe, Yasushi; Hidai, Masanobu |
Journal of publication | Journal of the Chemical Society, Dalton Transactions |
Year of publication | 2000 |
Journal issue | 20 |
Pages of publication | 3546 |
a | 9.951 ± 0.001 Å |
b | 10.3826 ± 0.0008 Å |
c | 12.707 ± 0.001 Å |
α | 87.707 ± 0.008° |
β | 87.033 ± 0.009° |
γ | 77.443 ± 0.007° |
Cell volume | 1279.17 ± 0.19 Å3 |
Cell temperature | 296.2 K |
Ambient diffraction temperature | 296.2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0233 |
Residual factor for significantly intense reflections | 0.0233 |
Weighted residual factors for significantly intense reflections | 0.0232 |
Weighted residual factors for all reflections included in the refinement | 0.0232 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.52 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7009929.html
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