Information card for entry 7009953

Structure parameters

• Formula: C24 H28 F3 N2 O3 P Pd S
• Calculated formula: C24 H28 F3 N2 O3 P Pd S
• SMILES: C(F)(S(=O)(=O)[O-])(F)F.[P]([Pd]1([n]2c3c(ccc2)ccc2c3[n]1ccc2)(C)(C)C)(C)(c1ccccc1)C
• Title of publication: Trimethyl-palladium(IV) and -platinum(IV) complexes containing phosphine donor ligands, including studies of 1,5,9-triethyl-1,5,9-triphosphacyclodecane and X-ray structural studies of palladium(II) and palladium(IV) complexes †
• Authors of publication: Bayler, Angela; Canty, Allan J.; Edwards, Peter G.; Skelton, Brian W.; White, Allan H.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 19
• Pages of publication: 3325
• a: 8.364 ± 0.001 Å
• b: 11.493 ± 0.002 Å
• c: 13.86 ± 0.002 Å
• α: 90°
• β: 105.812 ± 0.002°
• γ: 90°
• Cell volume: 1281.9 ± 0.3 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 8
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.043
• Residual factor for significantly intense reflections: 0.034
• Weighted residual factors for all reflections: 0.043
• Weighted residual factors for all reflections included in the refinement: 0.042
• Goodness-of-fit parameter for all reflections: 1.22
• Goodness-of-fit parameter for all reflections included in the refinement: 1.279
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No